Project Summary
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Project Information
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In this project, we present the procedure used for
developing a functional emulsion reactor with the
ability to control particle size through process
parameter optimization. This was accomplished
through the application of emulsion theory for the
determination of proper compound selection, vessel
composition analysis, critical micelle
concentration (CMC) theory analysis, mixing
analysis, subsurface-feeding flow analysis, and
particle size optimization testing. For this
project, a Chemglass 10 L jacketed reactor vessel
was fitted to a designed, Zinc-coated steel rigging
to house the emulsion. Agitation was accomplished
through the use of a MixerDirect
3Hp high output motor coupled with a Morehouse
Cowles 3 in. high shear mixing blade. A subsurface
oil phase feeding system was designed to deliver
oil to the high shear mixing region within the
vessel. Particle size optimization testing showed
the process parameter effects on particle size
distributions. Using the emulsion reactor, an
average particle size of less than 10microns with a
deviation of 5microns above and below the average
was determined. The optimal conditions for the
emulsion reactor were determined from a back-up
plan and implemented.
Emulsion Reactor
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Project Name
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Emulsion Reactor
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Project Number
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P13622
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Start Term
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2012-1
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End Term
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2012-3
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Faculty Guide
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Neal Eckhaus, neckhaus@gmail.com
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Primary Customer
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Mike Sanchez, Christiaan Richter
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Sponsor (financial support)
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RIT ChemE Department, Christiaan Richter
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Team Members
Stephen Heisler, John Miller, Ryan Foringer, Curtis
Williamson
Table of Contents
Acknowledgements